Marubeni has been granted a patent for a method to produce copper-selenide nanoparticles. The process involves forming flowable precursors, combining them in a lower-polarity solvent, and isolating the nanoparticles in an oxygen-depleted environment using a higher-polarity solvent. The method utilizes a segmented flow process for efficient production. GlobalData’s report on Marubeni gives a 360-degree view of the company including its patenting strategy. Buy the report here.
According to GlobalData’s company profile on Marubeni, Fuel cell powered drones was a key innovation area identified from patents. Marubeni's grant share as of March 2024 was 46%. Grant share is based on the ratio of number of grants to total number of patents.
Method for producing copper-selenide nanoparticles using flow process
A recently granted patent (Publication Number: US11897766B2) discloses a method for producing copper-selenide nanoparticles through a flow process. The method involves combining a copper starting material and a ligand to form a flowable copper precursor, suspending a selenium starting material in a liquid to form a flowable selenium precursor, and then combining these to create a flowable copper-selenium mixture in a lower-polarity solvent. By conducting a segmented flow of this mixture through heating units and isolating the nanoparticles in an oxygen-depleted environment using a deoxygenated, higher-polarity solvent, the process results in the production of copper-selenide nanoparticles.
Furthermore, the patent details various aspects of the method, including the use of a lower-polarity solvent in combining the copper starting material and ligand, the inclusion of an amine ligand in the flowable copper-selenium mixture, and the specific conditions for isolating the nanoparticles in an oxygen-depleted environment. The method also involves sparging both the copper and selenium precursors with a non-reacting gas to remove dissolved oxygen, along with sparging the deoxygenated higher-polarity solvent to ensure the removal of oxygen. Overall, the patented method offers a detailed and systematic approach to producing copper-selenide nanoparticles through a flow process, highlighting the importance of specific solvents, ligands, and environmental conditions in achieving successful nanoparticle synthesis.
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